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ChemicalBook >> CAS DataBase List >>5-Methoxyindole

5-Methoxyindole

CAS No.
1006-94-6
Chemical Name:
5-Methoxyindole
Synonyms
5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole
CBNumber:
CB4223553
Molecular Formula:
C9H9NO
Molecular Weight:
147.17
MDL Number:
MFCD00005674
MOL File:
1006-94-6.mol
MSDS File:
SDS
Last updated:2023-11-16 17:07:08

5-Methoxyindole Properties

Melting point 52-55 °C (lit.)
Boiling point 176-178 °C/17 mmHg (lit.)
Density 1.1135 (rough estimate)
refractive index 1.5310 (estimate)
Flash point 176-178°C/17mm
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Chloroform, Methanol
pka 16.70±0.30(Predicted)
form Crystalline Powder
color White to light brownish
Water Solubility insoluble
Sensitive Light Sensitive
BRN 116722
InChIKey DWAQDRSOVMLGRQ-UHFFFAOYSA-N
CAS DataBase Reference 1006-94-6(CAS DataBase Reference)
EWG's Food Scores 1
FDA UNII DQM3AS43PQ
NIST Chemistry Reference 1H-Indole, 5-methoxy-(1006-94-6)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P264-P271-P280-P302+P352-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36-24/25-37/39
WGK Germany  3
RTECS  NL9500000
8
Hazard Note  Irritant
HazardClass  IRRITANT, KEEP COLD, LIGHT SENSITIVE
HS Code  29339900
NFPA 704
1
2 0

5-Methoxyindole price More Price(31)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich M14900 5-Methoxyindole 99% 1006-94-6 1g $25 2023-06-20 Buy
Sigma-Aldrich M14900 5-Methoxyindole 99% 1006-94-6 5g $34 2023-06-20 Buy
TCI Chemical M0731 5-Methoxyindole >99.0%(GC) 1006-94-6 1g $32 2023-06-20 Buy
TCI Chemical M0731 5-Methoxyindole >99.0%(GC) 1006-94-6 5g $55 2023-06-20 Buy
Alfa Aesar B25290 5-Methoxyindole, 99% 1006-94-6 1g $41 2023-06-20 Buy
Product number Packaging Price Buy
M14900 1g $25 Buy
M14900 5g $34 Buy
M0731 1g $32 Buy
M0731 5g $55 Buy
B25290 1g $41 Buy

5-Methoxyindole Chemical Properties,Uses,Production

Chemical Properties

white to light brownish crystalline powder

Uses

5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.

Preparation

The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.

Definition

ChEBI: 5-methoxyindole is a member of indoles.

Reactions

5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.

Synthesis Reference(s)

Journal of Heterocyclic Chemistry, 26, p. 1405, 1989 DOI: 10.1002/jhet.5570260533
The Journal of Organic Chemistry, 58, p. 5558, 1993 DOI: 10.1021/jo00072a052
Tetrahedron Letters, 27, p. 837, 1986 DOI: 10.1016/S0040-4039(00)84114-3

Purification Methods

Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]

845619-77-4
1006-94-6
Synthesis of 5-Methoxyindole from 1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl-
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View Lastest Price from 5-Methoxyindole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
5-Methoxyindole pictures 2023-11-16 5-Methoxyindole
1006-94-6
US $129.00-645.00 / g 1g 0.99 25kg Shanghai UCHEM Inc.
5-Methoxyindole pictures 2023-07-25 5-Methoxyindole
1006-94-6
US $20.00-10.00 / kg 1kg 99% 2T Hebei Yanxi Chemical Co., Ltd.
5-Methoxyindole pictures 2023-03-27 5-Methoxyindole
1006-94-6
US $25.00 / KG 1KG 0.99 5000KG/MONTH XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
  • 5-Methoxyindole pictures
  • 5-Methoxyindole
    1006-94-6
  • US $20.00-10.00 / kg
  • 99%
  • Hebei Yanxi Chemical Co., Ltd.
  • 5-Methoxyindole pictures
  • 5-Methoxyindole
    1006-94-6
  • US $25.00 / KG
  • 0.99
  • XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
Methoxyindole 99% indol-5-yl methyl ether 5-Methoxyindole ,98% 5-METHOXYINDOLE (5MeOI) 5-methoxy-1H-indole(SALTDATA: FREE) 5-MethoxyindoleF 5-METHOXYINDOLE REPANIDAL NSC 521752 5-METHOXYINDOLE AKOS JY2082918 5-METHOXY-1H-INDOLE RARECHEM AH BS 0117 5-Methoxyindole in stock Factory TIMTEC-BB SBB004094 1H-Indol-5-yl methyl ether 5-methoxy-indol Femedol Indole, 5-methoxy- Methoxy-5 indole methoxy-5indole 5-Methyoxy Indole 5-methyloxyl indole 5-Methoxylindole Methoxyindole,99% Indol-5-yl methyl ether 5-Methoxyindole> 5-Methoxyindole 1006-94-6 1006-94-6 Indoles Simple Indoles Building Blocks Heterocyclic Building Blocks blocks IndolesOxindoles Heterocycles Indoles and derivatives IndoleDerivative Pyrroles & Indoles Heterocyclic Compounds Indole Series Indoles Indoline & Oxindole Indole Building Blocks C7 to C9 Chemical Synthesis Heterocyclic Building Blocks Heterocycle-Indole series Indole Derivatives Simple Indoles Chiral Compound Pyrroles & Indoles Building Blocks Heterocyclic Building Blocks
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